Optimisation of activated carbon production from date pits Online publication date: Sun, 09-Jun-2013
by Mohammed Hussein Essa; Muhammad A. Al-Zahrani; Suresh Nesaratnam
International Journal of Environmental Engineering (IJEE), Vol. 5, No. 3, 2013
Abstract: This study investigates the optimal process conditions for activated carbon production from local date palm pits using response surface methodology (RSM). Box Behnken statistical technique was used to design the production process in order to determine the influence of activation temperature (300°C to 700°C), % H3PO4 (30% to 70%) and activation time (1 to 3 hours) on the BET surface area. Second-order model developed via regression analysis to describe the BET surface area response was found to be appropriate in predicting the responses within the experimental region to a considerable extent. Analysis of variance (ANOVA) revealed that the influence of the independent variables on the BET surface area is in the order: activation temperature > % H3PO4 > activation time with only temperature and % H3PO4 possessing moderate interaction. The maximum BET surface area from RSM optimisation was estimated to be 1,337.54.2 m²%g achievable at optimum conditions of 54% H3PO4 and 547°C carbonisation temperature at an activation time of 2.067 hours.
Online publication date: Sun, 09-Jun-2013
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