Silica with grafted silicon hydride groups and its application for preparation of palladium nanoparticles
by N.A. Ivashchenko; K.V. Katok; V.A. Tertykh; V.V. Yanishpolskii; S.A. Khainakov
International Journal of Nanoparticles (IJNP), Vol. 4, No. 4, 2011

Abstract: Chemically modified silica containing ?SiH groups were used for the synthesis of palladium nanoparticles by reduction of palladium nitrate solution in mild conditions. Thermogravimetric analysis and IR-spectroscopy were applied for characterisation of hydridesilica and for studying of a process of formation of palladium nanoparticles. For the confirmation of metal particles formation X-ray diffraction, UV-vis spectroscopy and transmission electron microscopy (TEM) were used.

Online publication date: Fri, 13-Mar-2015

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