Title: Synthesis and characterisation of nanostructured barium cuprate thin films

Authors: M. Faiz, N. Tabet

Addresses: Surface Science Laboratory, Physics Department, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi Arabia. ' Surface Science Laboratory, Physics Department, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi Arabia

Abstract: Thin films of Ba1−y CuO2+x system were prepared by DC magnetron sputtering technique, using a BaCuO2 target sintered at 850°C for 24 hours. The sputtering was performed under 0.04 Torr Ar-pressure and at 500 V-135 mA target current. The effect of substrate and substrate bias on the morphology of the films was investigated. The films were characterised by atomic force microscopy (AFM), X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS). The XRD and XPS analyses revealed a major phase closed to BaCuO2 as well as a minor phase of BaCO3 (30%). AFM observations in the phase mode showed a uniform distribution of isolated grains covering about 30% of the film. We identified these grains with BaCO3. The AFM images in the topography mode showed a uniform distribution of 60 nm diameter grains of BaCuO2.

Keywords: barium cuprate; nanostructures; thin films; atomic force microscopy; AFM; X-ray photoelectron spectroscopy; XPS; X-ray diffraction; XRD; DC magnetron; nanomaterials; nanotechnology.

DOI: 10.1504/IJNBM.2009.027717

International Journal of Nano and Biomaterials, 2009 Vol.2 No.1/2/3/4/5, pp.234 - 239

Published online: 08 Aug 2009 *

Full-text access for editors Full-text access for subscribers Purchase this article Comment on this article