Microwave-assisted synthesis of size-controlled silver nanoparticles using polyvinyl pyrrolidone as a reducing agent
by Yonghui Song; Jiating Zhou; Xinzhe Lan
International Journal of Nanomanufacturing (IJNM), Vol. 10, No. 1/2, 2014

Abstract: In this work, stable concentrated aqueous dispersions of size-controlled silver nanoparticles were prepared by microwave irradiation of silver nitrate (AgNO3)/polyvinyl pyrrolidone (PVP) solution using polyvinyl pyrrolidone (PVP) as a reducing and stabilising agent. Crystal structure, size, optical properties of the silver nanoparticles were characterised by means of X-ray diffraction (XRD), scanning electron microscope (SEM), ultraviolet visible spectroscopy (UV-vis), Fourier transform infrared (FT-IR). Quasi-spherical nanoparticles, nanocube and flake-like nanoparticles were synthesised by controlling the experimental parameters such as the ratio of PVP to AgNO3, and the particle size can be conveniently adjusted to 50 nm.

Online publication date: Sat, 17-May-2014

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